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Getzler Lab at KenyonCollege

It’s spring break for my kids, but not me, so my wife went with them to CA to visit family. That means I get to spend all of my 48th birthday in lab metalating a ligand and recrystalizing a complex. It feels so good to use the skills I spent so many years building

Clear, colorless solvent boiling under vacuum in a round bottomed flask
Nitrogen boiling out of a Dewar flask as solvent condenses in the trap of a vacuum manifold. The cold boiling gas flows downward and condenses water vapor, which is visible
I middle aged whiteish-looking man wearing safety glasses and a flame resistant lab coat gives a thumbs up, standing in front of a Schlenk line
Apr 09, 2023, 07:22 PM·Public·Mastodon for iOS
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Getzler Lab at KenyonCollege

Excellent yield and packed up for use!
Synthesis from doi.org/10.1021/ma400046x

White powder at the bottom of a round bottomed flask. Stir bar taped to the side with yellow tape
White powdered in a crimped aluminum weigh boat. Photo taken through the window of an inert atmosphere glove box
A bulky black rubber glove holding a 20 mL glass vial with a green cap containing a white powder. Vial labeled “(tBuSalAmEE)Al YDG-3-003 4/10/23 tare w/cap: 18.200 g”
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